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本文对Ｃｏ（ＢＰＨ＿４）＿２．８Ｈ＿２Ｏ的合成及脱水、氧化分解过程进行了研究，给出了脱水温度及脱水过程的动力学参数，并对氧化分解机理进行了分析讨论。
In this paper, the synthesis, dehydration and oxidative decomposition of Co (BPH_4) _2.8H_2O were studied. The dehydration temperature and the kinetic parameters of dehydration process were given. The oxidation and decomposition mechanism was also discussed.