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A novel supramolecular adduct 3(C 42H 42N 28O 14) 2·H 2O (1) was synthesized by mixing 2- and cucurbit uril in solution of hydrochloric acid. The crystal structure was determined by single crystal X-ray diffraction analysis. The crystal belongs to orthorhombic system and space group F dd2 with cell dimensions: a=4.705 33 (5) nm, b=7.153 80 (6) nm, c= 1.894 61 (2) nm, Z=16, V=63.7744 (11) nm3, D c= 1.534 g/cm3, μ=3.007 mm -1, F(000)=29 120, R 1= 0.070 7, wR 2=0.169 2. In crystal, the cucurb uril molecules form two zig-zag chains.
A novel supramolecular adduct 3 (C 42H 42N 28O 14) 2 · H 2O (1) was synthesized by mixing 2- and cucurbit uril in solution of hydrochloric acid. The crystal structure was determined by single crystal X-ray diffraction analysis. The crystal b = 7.153 80 (6) nm, c = 1.894 61 (2) nm, Z = 16, V = 63.7744 (11) In the orthorhombic system and space group F dd2 with cell dimensions: nm3, D c = 1.534 g / cm 3, μ = 3.007 mm -1, F (000) = 29 120, R 1 = 0.070 7, wR 2 = 0.169 2. In crystal, the cucurb uril molecules form two zig-zag chains .