Preparation and Characterization on Nano- Sized Barium Titanate Powder Doped with Lanthanum by Sol-G

来源 :Journal of Rare Earths | 被引量 : 0次 | 上传用户:tangdongd
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The nano-sized BaTiO3:La3+ powders were prepared by sol-gel process using butyl phthalate, barium acetate and lanthanum oxide as raw material, and these samples were tested by means of TG-DTA, XRD and SEM. The results indicate that with the annealing temperature and the doped concentration rising, the powders’ particle sizes will increase and decrease respectively. When annealing temperature is 900℃and doped concentration is 7%, the phase is cubic without other phases, and the particle size of power is 43 .34 nm. The nano-sized BaTiO3: La3 + powders were prepared by sol-gel process using butyl phthalate, barium acetate and lanthanum oxide as raw material, and these samples were tested by means of TG-DTA, XRD and SEM. The results indicate that with the the annealing temperature and the doped concentration rising, the powders’ particle sizes will increase and decrease respectively. When annealing temperature is 900 ° C. and the concentration of doped is 7%, the phase is cubic without other phases, and the particle size of power is 43 .34 nm.
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