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The title compound was synthesized and characterized by means of elemental analysis, IR, DTA-TG and UV. Its single crystal structure was solved by using direct methods. The compound crystallizes in the orthorhombic space group Pmc(?) with lattice parameters: a = 1. 7261(2), b=l. 7537(3), c=2. 4258(3) nm. V=7. 34220 nm3, F(000) = 3648, Z = 4. The structure was refined to conventional discrepancy factors of R=0. 060 for 3176 observed reflections [Ⅰ>3σ/(Ⅰ)]. The anion represents a modification of the well-known [Mo6O19]2- anion, in which a single terminal oxo group is replaced by a 2,4-dinitrophenyl hydrazine ligand while the structure integrity of the hexanuclear framework is maintained.
The single crystal structure was solved by using direct methods. The compound crystallizes in the orthorhombic space group Pmc (?) With lattice parameters: a = 1.7261 (2), b = 1.7537 (3), c = 2.4258 (3) nm. V = 7.34220 nm3, F (000) = 3648, Z = 4. The structure was refined to conventional discrepancy factors of R = 0. 060 for 3176 observed reflections [I> 3σ / (I)]. The anion represents a modification of the well-known [Mo6O19] 2- anion, wherein a single terminal oxo group is replaced by a 2,4-dinitrophenyl hydrazine ligand while the structure integrity of the hexanuclear framework is maintained.