[目的]对4-甲氧基苯酚催化加氢制备4-甲氧基环己酮的工艺路线进行优化。[方法]以对4-甲氧基苯酚为原料,通过催化加氢制备4-甲氧基环己酮。[结果]在反应温度100℃,氢气压力0.8 MPa,底物浓度25%条件下,4-甲氧基环己酮最高摩尔收率达到95.3%,实验室自制Pd/C催化剂套用4次后,活性与选择性均无明显下降。 [Objective] The optimization of 4-methoxy-cyclohexanone catalytic hydrogenation process was optimized. [Method] With 4-methoxyphenol as raw material, 4-methoxycyclohexanone was prepared by catalytic hydrogenation. [Result] The maximum molar yield of 4-methoxycyclohexanone reached 95.3% under the condition of reaction temperature of 100 ℃, hydrogen pressure of 0.8 MPa and substrate concentration of 25%. After self-made Pd / C catalyst was applied for 4 times, No significant decrease in activity and selectivity.