Study on Preparation of ~(93)Zr AMS Standards——Separation of Zr-Nb by Solvent Extraction with HDEHP

来源 :Annual Report for China Institute of Atomic Energy | 被引量 : 0次 | 上传用户:markwolf
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The zirconium isotope ~(93)Zr with a half-life of 1.5×10~6 is produced by nuclear fission and neutronactivation of the stable isotope ~(92)Zr. The measurement of ~(93)Zr can be used for the treatment of nuclearwaste and the influence on environment of fission product. AMS is a kind of relative measurement withhigh sensitivity, which requires standard samples, and furthermore, the isobaric interference of ~(93)Nb isstrong, so we developed a chemical separation procedure to reduce the content of Nb during thepreparation of standards. A solvent extraction method is presented for the separation of Zr from Nb. During the course of The zirconium isotope ~ (93) Zr with a half-life of 1.5 × 10 ~ 6 is produced by nuclear fission and neutron activation of the stable isotope ~ (92) Zr. The measurement of ~ (93) Zr can be used for the treatment of nuclear waste and the influence on environment of fission product. AMS is a kind of relative measurement with high sensitivity, which requires standard samples, and further, the isobaric interference of ~ (93) Nb isstrong, so we developed a chemical separation procedure to reduce the content of Nb during the preparation of standards. A solvent extraction method is presented for the separation of Zr from Nb. During the course of
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