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目的:建立1种银丹心泰滴丸中天然冰片的气相色谱法含量测定方法。方法:采用HP-INNOWAX(30.0 mm×0.25 mm,0.25μm)色谱柱,柱温为135℃,进样口温度为235℃,FID检测器温度为255℃;测定银丹心泰滴丸中天然冰片的含量。结果:冰片质量浓度在0.2~2.5 mg/mL范围内,具有良好的线性关系(r~2=0.999 2,n=6),加样平均回收率为99.43%,RSD=1.25%(n=9),3批样品中冰片含量平均为0.44 mg/丸。结论:本法简单、准确、重复性好,可以作为银丹心泰滴丸中冰片的定量方法。
Objective: To establish a method for determination of natural borneol in Yindanxintaidi pill by gas chromatography. Methods: HP-INNOWAX (30.0 mm × 0.25 mm, 0.25 μm) column was used. The column temperature was 135 ℃, the inlet temperature was 235 ℃ and the FID detector temperature was 255 ℃. Content. Results: The average linear recovery (r2 = 0.999 2, n = 6) of borneol in the range of 0.2-2.5 mg / mL was 99.43% and the RSD was 1.25% (n = 9 ), The average amount of borneol in three batches of samples was 0.44 mg / pill. Conclusion: The method is simple, accurate and reproducible. It can be used as a quantitative method for borneol in Yindanxintai pills.