Preparation and performance of CeO_2 hollow spheres and nanoparticles

来源 :Journal of Rare Earths | 被引量 : 0次 | 上传用户:wcj_lp
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CeO_2 hollow spheres were synthesized by polystryrene sphere(PS) templates and CeO_2 nanoparticles were prepared by a facile method. The as-obtained products were characterized by scanning electron microscopy(SEM), N_2 adsorption-desorption, X-ray diffraction(XRD), Fourier transform infrared spectroscopy(FTIR) and UV-vis diffuse reflectance spectra. The results showed that the structure of the obtained CeO_2 hollow spheres was hollow microsphere with a diameter of 380 nm and the average particle size of CeO_2 nanoparticles was about 1700 nm. The two samples’ Brunauer-Emmett-Teller(BET) surface area was 67.1 and 37.2 m~2/g. The CeO_2 hollow spheres had a better performance than nanoparticles at UV-shielding because of higher surface area and the structure of hollow sphere. CeO 2 hollow spheres were synthesized by polystryrene sphere (PS) templates and CeO 2 nanoparticles were prepared by a facile method. The as-obtained products were characterized by scanning electron microscopy (SEM), N 2 adsorption-desorption, X-ray diffraction Fourier transform infrared spectroscopy (FTIR) and UV-vis diffuse reflectance spectra. The results showed that the structure of the obtained CeO 2 hollow spheres was hollow microspheres with a diameter of 380 nm and the average particle size of CeO 2 nanoparticles was about 1700 nm. Two samples’ Brunauer-Emmett-Teller (BET) surface area was 67.1 and 37.2 m 2 / g. The CeO 2 hollow spheres had a better performance than nanoparticles at UV-shielding because of higher surface area and the structure of hollow sphere.
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