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Mr=299.8, triclinic, Pl, a=10.395(2), b=11.191(2), c=14.051(3)A, α=81.80(2), β=89.42(2), r=66.47(1)°, v=1481.4(5)A3, Z=4, μ(MoKα)=3.37 cm-1, F(000)=632, Dx=1.34 g/cm3, room temperature. The final R=0.058, with unit weights and s=1.33 for 2900 independent reflexions with |Fo| ≥2.5σ(|Fo|). There are two molecules in an asymmetric unit and the lengths of dative N→ Si bond for the two molecules are 2.185(4) and 2.177(4)A, respectively. The different conformations were observed due to the rotation of the chloro-methyl groups.
Mr = 299.8, triclinic, Pl, a = 10.395 (2), b = 11.191 (2), c = 14.051 (3) A,? = 81.80 (2),? = 89.42 (2), r = 66.47 The final R = 0.058, with unit weights, V = 1481.4 (5) A3, Z = 4, μ (MoKα) = 3.37 cm -1, F (000) = 632, Dx = 1.34 g / cm 3, room temperature and s = 1.33 for 2900 independent reflexions with | Fo | ≥ 2.5σ (| Fo |). There are two molecules in an asymmetric unit and the lengths of dative N → Si bond for the two molecules are 2.185 (4) and 2.177 ( 4) A, respectively. The different conformations were observed due to the rotation of the chloro-methyl groups.