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By hydrothermal synthesis, a manganese(II) tetracarboxylate [Mn(2,2′-bipyridi- ne)(btec)0.5(H2O)]2n (H4btec = 1,2,4,5-benzenetetracarboxylic acid) was obtained and characteri- zed by single-crystal X-ray diffraction, IR, elemental analysis and thermogravi