水浴法制备蝴蝶状的微结构CuO

来源 :无机化学学报 | 被引量 : 0次 | 上传用户：huangpeifei

【摘要】

：

以硝酸铜为铜源,六次甲基四胺为有机碱,去离子水为溶剂,采用简捷水浴加热技术控制合成了由三角纳米片组成的蝴蝶状微结构CuO.产品的组成和形貌用XRD、EDX、场发射扫描电镜(FE

【作者】

：

胡寒梅邓崇海孙凤霞张克华孙梅宣寒

【机构】

：

安徽建筑工业学院材料与化学工程学院,安徽建筑工业学院先进建筑材料安徽省重点实验室,合肥学院化学与材料工程系

【出处】

：

无机化学学报

【发表日期】

：

2004年期

【关键词】

：

氧化铜微结构晶体生长水浴技术 copper oxide microstructure crystal growth water bath techniqu

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论文部分内容阅读

以硝酸铜为铜源,六次甲基四胺为有机碱,去离子水为溶剂,采用简捷水浴加热技术控制合成了由三角纳米片组成的蝴蝶状微结构CuO.产品的组成和形貌用XRD、EDX、场发射扫描电镜(FESEM) 、TEM、HRTEM和选区电子衍射(SAED)进行了表征.结果表明CuO的形貌主要受六次甲基四胺用量的影响.随着其用量的增加,CuO的形貌经历了飞鱼状-蝴蝶状-牡丹状的递变.并对蝴蝶状CuO微结构的形成机制及形貌的演变进行了探讨.

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水浴法制备蝴蝶状的微结构CuO

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