在相对较低的温度下,以蔗糖为碳源,Ni-Fe(Ni/Fe=2)双层氢氧化物作为催化剂前驱体和模板,通过固相法制备石墨化介孔炭。通过X射线衍射仪(XRD)、透射电子显微镜(TEM)和拉曼光谱法(Raman)对产物的结构和形貌进行表征。结果显示该材料具有较高的石墨化程度。氮气吸附和孔径分布显示制备出的石墨化炭的孔径分布均匀;同时,对石墨化炭的形成过程进行了分析。 Graphite mesoporous carbon was prepared by solid phase method at a relatively low temperature using sucrose as carbon source and Ni-Fe (Ni / Fe = 2) double hydroxide as catalyst precursor and template. The structure and morphology of the product were characterized by X-ray diffraction (XRD), transmission electron microscopy (TEM) and Raman spectroscopy (Raman). The results show that the material has a high degree of graphitization. Nitrogen adsorption and pore size distribution showed that the pore size distribution of graphitized carbon prepared was uniform. Meanwhile, the formation of graphitized carbon was also analyzed.