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A novel dimeric complex [Ru3Ⅲ,Ⅲ,Ⅱ(μ3-O)(μ-CH3COO)(CO)]2(μ-dppf)(μ-odppf) (dppf =1, l′-bis(diphenylphosphio)ferrocene, odppf = 1, 1′-bis(oxodiphenylphosphoranyl)ferrocene) (1) of oxo-centered triruthenium-aectate cluster units was synthesized and character