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1-苯甲酰基-3-芳基硫脲与氯乙酰氯反应合成了1-芳基-3-苯甲酰基-2-硫代咪唑啉-4-酮,与二氯乙酰氯反应合成了1-芳基-3-苯甲酰基-5-氯-2-硫代咪唑啉-4-酮,与三氯乙酰氯反应时仅得到了硫脲的分解重组产物苯甲酰基芳胺.产物结构经红外光谱、核磁共振谱和高分辨质谱表征.
Synthesis of 1-aryl-3-benzoyl-2-thioimidazolidin-4-one by 1-benzoyl-3-arylthiourea with chloroacetyl chloride and 1 -Aryl-3-benzoyl-5-chloro-2-thioimidazolidin-4-one, with only trichloroacetyl chloride obtained only the decomposition reaction of thiourea benzoylarylamine. Infrared spectroscopy, nuclear magnetic resonance spectroscopy and high resolution mass spectrum characterization.