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芳香硫醇、芳香或脂肪二硫化物溶于二氯甲烷,在三甲基氯硅烷-硝酸盐的作用下50℃反应,得到相应的磺酰氯。13例收率85%～98%。
Aromatic thiols, aromatic or aliphatic disulfides are dissolved in methylene chloride and reacted with trimethylchlorosilane-nitrate at 50 ° C to give the corresponding sulfonyl chlorides. 13 cases of the yield of 85% to 98%.