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对陶瓷-金属封接的“玻璃状”的相互作用的相位中的失透现象进行了研究,以论证促进结晶生长的条件并找出微观结构上的这种变化与封接强度之间的关系。这一现象首先是在典型的陶瓷和金属化系统中加以研究的,因为大量的实验数据如相平衡关系、熔融物粘度、陶瓷微观结构、表面能量关系、热膨胀以及烧结特性等对其是有价值的。为了促进失透,金属化的陶瓷被热处理、装架、作机械强度试验并用X-射线衍射检查进行第二结晶相的数量的半定量测定。失透性能完全符合相平衡理论。强度数据表明与失透关系不大。本研究概述了金属化系统的生产,并且为了检查样品,还采用了电子显微镜和电子探针微量分析仪器。
The devitrification phenomenon in the phase of the “glassy” interaction of the ceramic-metal seal was investigated to demonstrate the conditions that promote crystal growth and to find out the relationship between this change in microstructure and the strength of the seal . This phenomenon was first investigated in typical ceramic and metallization systems because of the value of a large number of experimental data such as phase equilibrium, melt viscosity, ceramic microstructure, surface energy relationships, thermal expansion, and sintering properties of. In order to promote devitrification, the metallized ceramic was heat treated, rack mounted, subjected to mechanical strength tests and subjected to semi-quantitative determination of the number of second crystalline phases by X-ray diffraction examination. Loss of performance in full compliance with phase equilibrium theory. Intensity data show little relationship with devitrification. This study outlines the production of metallization systems and, for the purpose of examining the samples, electron microscopy and electron probe microanalysis equipment.