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A metal-organic framework,[Mn2(PDC)2(2,2-bpy)2(H2O)2]n·2nH2O (1) (H2PDC =pyridine-3,4-dicarboxylie acid,2,2-bpy =2,2-bipyribine),has been synthesized under hydrothermal conditions and characterized by elemental analysis and single crystal X-ray diffraction.Compound (1) presents a two-dimensional structure and exhibits intense fluorescent emission upon photo-excitation.