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By using the chemical and physical method of pre-treating from the cellulose mostly,the research on Bio mass converts to the glucose.the manufacture study that issues this and generates the ethanol or the bio butanol is the majority.This biological phosphorus method has the advantage that the selectivity is high.But the overall yield of the ethanol is low.There is lots of the energy consumption and the problem that there is the limit is in the profitability according to each process.This research the low molecularizaion of the cellulose which uses the new radical catalytic reaction in order to overcome the limit of this biological progress and methanol formation was progressed with the object In this research,it confirmed that it became the time and the cellulose analyze the condensation (Top product) generated in the condenser of the residue which it remains in the bottom part of the evaporator through the evaporator which directly it makes by using the methyl cellulose and hydrogen peroxide and iron catalyst (Bottom product) and upper part with HPLC and GC-MS with I differentiation.It confirmed that methanol was generated in the generated condensation (Top product).