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ＣＳ＿２在Ｃｕ─Ｓ键中插入产物（Ｐｈ＿３Ｐ）＿２Ｃｕ（Ｓ＿２ＣＳＲ）（Ｒ＝Ｂｕ￣ｔ或与丙酮－Ｐｙ混合溶剂反应，获得了双核铜化合物［ＣｕＩ（ＰＰｈ＿３）（Ｐｙ）］＿２和［ＣＨ＿２（Ｃ＿５Ｈ＿５Ｎ）＿２］＿２［Ｃｕ＿２Ｉ＿６］两个化合物晶体，用Ｘ射线单晶衍射法测得它们的晶体结构。
CS_2 was synthesized by the insertion of the product (Ph_3P) _2Cu (S_2CSR) into the Cu-S bond (R = Bu ~ t or reaction with acetone-Pyyridine solvent to obtain the dinuclear copper compound [CuI (PPh_3) (Py)] _2 and [CH_2 C_5H_5N) _2] _2 [Cu_2I_6] two crystal compounds, their crystal structures were measured by X-ray single crystal diffraction.