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A poly(tert-butyl methacrylate)(PBMA) macromonomer was synthesized by anionic polymerization with bis(2,6-di-t-butyl phenoxy) methyl aluminum [MeAl(ODBP)2] as the initiator and trimethylsilylmethacrylate(TMSMA) as the end capping agent in dry THF. Then, a