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At room temperature,a coordination polymer [Ni(btec)(H2O)4][Ni(imi)2(H2O)4]·2H2O was synthesized by reaction of NiCl2·6H2O,1,2,4,5-benzenetetracarboxylic dianhydride and imidazole in a water/THF solution.The structure was determined by X-ray dif