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A new molecular conductor (PyH)[Ni(dmit)2]2 (dmit = 4, 5-dimercapto-1, 3-dithiole-2-thione) has been prepared and its crystal structure has been determined. Crystallographicparameters for (PyH)[Ni(dmit)2]2: C17H6NNi2S20; triclinic system; P-1 space group;