Synthesis and surface modification of the nanoscale cerium borate as lubricant additive

来源 :Journal of Rare Earths | 被引量 : 0次 | 上传用户:jay1222
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Nanoparticle of cerium borate with a size of about 50 nm was synthesized via sol-gel precipitation method under micro-emulsion by oleic acid,using Na2B4O7 and Ce(NO3)3 aqueous solution as raw materials,and the morphology and microstructure of as-prepared particles were characterized by means of scanning electron microscopy(SEM) equipped with an energy-dispersive X-ray spectrometer(EDS),X-ray diffraction(XRD),infrared spectroscopy(IR),and thermogravimetric analysis(TGA).Two methods to disperse the particles into base oil were employed,and the results derived from the four-ball tribotester indicated that the friction coefficient of the base oil by the addition of the nanoscale cerium borate particles diminished greatly,and the anti-wear properties also depended on the dispersion methods. Nanoparticle of cerium borate with a size of about 50 nm was synthesized via sol-gel precipitation method under micro-emulsion by oleic acid, using Na2B4O7 and Ce (NO3) 3 aqueous solution as raw materials, and the morphology and microstructure of as-prepared Particles were characterized by means of scanning electron microscopy (SEM) equipped with an energy-dispersive X-ray spectrometer (EDS), X-ray diffraction (XRD), infrared spectroscopy (IR), and thermogravimetric analysis (TGA) disperse the particles into base oil were employed, and the results derived from the four-ball tribotester indicated that the friction coefficient of the base oil by the addition of the nanoscale cerium borate particles diminished greatly, and the anti-wear properties also depended on the dispersion methods.
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