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The reaction of tricyanometallate precursor,Bu4N[Fe(Tp)(CN)3] and (Bu4N)[(pzTp)Fe(CN)3] (Tp =tris(pyrazolyl)hydroborate,pzTp =tetrakis(pyrazolyl)borate) with Ni(ClO4)2·6H2O in the presence of the monodentate N-methylimidazole ligand afforded two new