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利用正丙醇锆受控水解方法制备ＹＳＺ粉．研究在正丙醇锆－硝酸钇－乙酰丙酮体系中，Ａｃａｃ／Ｚｒ（ｍｏｌ），Ｈ２Ｏ／Ｚｒ（ｍｏｌ）对正丙醇锆水解影响．采用ＴＧ－ＤＴＡ，ＸＲＤ，Ｒａｍａｎ光谱，ＢＥＴ，ＴＥＭ等手段对ＹＳＺ粉体进行表征．发现本体系获得的粉体立方相成相温度可低至３５０℃，颗粒度在１０ｎｍ左右
YSZ powder was prepared by controlled hydrolysis of zirconium n-propoxide. The effects of Acac / Zr (mol) and H 2 O / Zr (mol) on the hydrolysis of zirconium n-propoxide were investigated in the system of n-propoxide zirconium-yttrium nitrate-acetylacetonate. YSZ powder was characterized by TG-DTA, XRD, Raman spectroscopy, BET and TEM. It is found that the cubic phase temperature of the powder obtained from this system can be as low as 350 ° C and the particle size is about 10 nm