【摘 要】
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A novel metal-organic coordination polymer [Cu2(phen)(ipt)2]2n·nH2O 1 has been hydrothermally synthesized and structurally characterized by single-crystal X-ra
【机 构】
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Jilin Normal University,Department of Chemistry
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A novel metal-organic coordination polymer [Cu2(phen)(ipt)2]2n·nH2O 1 has been hydrothermally synthesized and structurally characterized by single-crystal X-ray diffraction. The complex crystallizes in monoclinic, space group P21/c with a = 12.338(3), b = 12.167(3), c = 18.167(4)(A), β = 111.686(14)o, V = 2534.1(10) A)3, C28H18Cu2N2O9, Mr = 653.52, Dc = 1.713 g/cm3, μ(MoKα) = 1.740 mm-1, F(000) = 1320, Z = 4, the final R = 0.0443 and wR = 0.0853 for 3543 observed reflections (I > 2σ(I)). It exhibits a novel two-dimensional network with tetra- Cu-ipt- as building units.
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