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我们用多孔层玻璃毛细管柱进行了烷基化油的分析方法研究。实验条件: 仪器:用SP—2305气相色谱仪改装成毛细管色谱仪。在汽化室后增设了分流系统,利用载气线路一路作分析柱使用,另一路为补加气。氢火焰鉴定器,记录仪满量程10mV,笔速1秒,记录纸1cm/分。色谱柱:柱长82米,内径0.25毫米,天津试剂二厂产多孔层鲨鱼烷玻璃柱,使用前于80℃柱温下老化4小时,理论板数1200
We used porous glass capillary column for the analysis of alkylate oil. Experimental conditions: Instrument: Refined with a SP-2305 gas chromatograph into a capillary chromatograph. After the evaporation chamber additional diversion system, the use of carrier gas line all the way to the analytical column to use the other way to make up for gas. Hydrogen flame detector, full-scale recorder 10mV, pen speed of 1 second, recording paper 1cm / min. Column: 82 meters long column, an inner diameter of 0.25 mm, Tianjin Reagent Factory production porous layer shark alkyl glass column, before use at 80 ℃ for 4 hours at a column temperature, the theoretical plate number 1200