【摘 要】
：
Molybdenum(Ⅰ)-compound [Mo2(SC6H11)2(CO)8] 1, crystallizes in monoclinic, space group P21/c with a = 9.5863(9), b = 9.4469(9), c = 13.869(1) (A), β= 99.697(2)
【机 构】
：
State Key Laboratory of Structural Chemistry
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Molybdenum(Ⅰ)-compound [Mo2(SC6H11)2(CO)8] 1, crystallizes in monoclinic, space group P21/c with a = 9.5863(9), b = 9.4469(9), c = 13.869(1) (A), β= 99.697(2)o, V = 1238.1(2)(A)3, Z = 2, Dc = 1.734 g/cm3, μ= 12.23 cm-1 and F(000) = 644. The final R = 0.0455 and wR = 0.1159 for 1590 observed reflections with I > 2((I). 1 possesses a rhombic bimetallic core MoS2Mo with the Mo-Mo bond length of 2.975(1) and Mo-S of 2.485(2) (A).
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