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采用Ｍ ｓｓｂａｕｅｒ效应和ＸＲＤ分析方法研究了非晶合金Ｆｅ７３．１Ｃｕ３．２Ｎｂ３．２Ｓｉ１２．５Ｂ１０．０的晶化。实验表明，该非晶合金有两个晶化阶段。在第一阶段晶化后，样品主要由ＤＯ３型的ａ—ＦｅＳｉ合金的超细颗粒和作为晶界的非晶相两部分组成。随着退火温度的上升，晶化相的含量增加，非晶相含量减少、在第二阶段晶化后，残余的非晶相就晶化为Ｆｅ２Ｂ和Ｆｅ２３Ｂ６化合物以及可能为Ｆｅ－Ｎｂ－Ｂ之类的顺磁相。
The crystallization of amorphous alloy Fe73.1Cu3.2Nb3.2Si12.5B10.0 was studied by M ssbauer effect and XRD analysis. Experiments show that the amorphous alloy has two crystallization stages. After the first stage of crystallization, the sample mainly consists of ultrafine particles of DO3-type a-FeSi alloy and amorphous phase as a grain boundary. As the annealing temperature increases, the content of the crystallized phase increases and the amorphous phase content decreases. After the second stage of crystallisation, the residual amorphous phase crystallizes into Fe2B and Fe23B6 compounds and possibly Fe-Nb-B Paramagnetic class.