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In this work a new Lu3+ PVC-membrane sensor based on 2,2-dithiobis(4-methyIthiazole) (TMT) has been fabricated. The sensor exhibits a Nernstian slope of 19.6 ± 0.4 mV decade 1 in the concentration range of 1.0 × 10 6-1.0 × 10 2 mol L 1 and a detection limit of 6.8 × 10 7 mol L 1.It could work well in the pH range of 2.7-9.6. The selectivity of the sensor against a lot of common alkaline, alkaline earth, transition, heavy metals and specially lanthanide ions was very good.