RP-HPLC法测定生化丸中阿魏酸的含量

来源 :南京中医药大学学报 | 被引量 : 0次 | 上传用户:rongcs
下载到本地 , 更方便阅读
声明 : 本文档内容版权归属内容提供方 , 如果您对本文有版权争议 , 可与客服联系进行内容授权或下架
论文部分内容阅读
目的:为定量分析生化丸的质量提供有效手段。方法:用RP-HPLC法对生化丸中阿魏酸的含量进行测定。固定相为HYPERSILBDSC18柱,4.6(i.d.)×200mm;流动相为甲醇-5%冰醋酸水溶液(25∶75);检测波长为322nm。结果:2种成药阿魏酸含量最高为0.82mg/g;最低为0.44mg/g。结论:测定生化丸中阿魏酸含量对控制生化丸的质量有重要意义 Objective: To provide an effective method for quantitative analysis of the quality of Biochemical Pills. Methods: The contents of ferulic acid in Biochemical Pills were determined by RP-HPLC. The stationary phase was HYPERSILBDSC18 column, 4.6 (i.d.) × 200mm; the mobile phase was methanol-5% acetic acid aqueous solution (25:75); the detection wavelength was 322nm. Results: The highest content of ferulic acid in the two drugs was 0.82mg / g and the lowest was 0.44mg / g. Conclusion: Determination of biochemical pills ferulic acid content of the quality control of biochemical pills of great significance
其他文献
本文采用HPLC法测定正柴胡饮冲剂中芍药甙含量,方法简便,干扰较小,加样回收率达99.0%,RSD为2.74%。 In this paper, HPLC determination of paeoniflorin Zhengchaihu drink granules, the method
期刊