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Based on a 3-(pyridine-2-yl)-4H-1,2,4-triazole ligand(Hpytr), one 2D Cd(Ⅱ) coordination polymer [Cd I(pytr)]_n(1) and one 2D Mn(Ⅱ) coordination polymer [Mn(N_3)(pytr)(H_2O)]_n(2) have been synthesized and characterized by X-ray crystallography, elemental