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The title compound N-phenyl-2-deoxy-D-ribopyranosylamine featuring a single conformation and pyranose-ring has been synthesized and characterized by NMR spectrum and X-ray diffraction. X-ray crystal structure analysis shows that its crystal belongs to the monoclinic system, space group P21 with a = 6.5375(9), b = 7.7140(9), c = 10.7865(16) , β = 97.578(11)o, Z = 2, V = 539.22(13) 3, Dc = 1.289 g/cm3 , F(000) = 224, μ(MoKα) = 4.533 mm-1, R = 0.0305 and wR = 0.0639 for 1093 observed reflections (I > 2σ(I)). This compound exists as α-conformation and 1C4 chair-like configuration.
The title compound N-phenyl-2-deoxy-D-ribopyranosylamine featuring a single conformation and pyranose-ring has been synthesized and characterized by NMR spectrum and X-ray diffraction. X-ray crystal structure analysis shows that its crystal belongs to the monoclinic space group P21 with a = 6.5375 (9) b = 7.7140 (9) c = 10.7865 (16) β β = 97.578 (11) o Z = 2 V = 539.22 133 Dc = 1.289 g / cm3, F (000) = 224, μ (MoKα) = 4.533 mm -1, R = 0.0305 and wR = 0.0639 for 1093 observed reflections (I> 2σ (I) and 1C4 chair-like configuration.