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Melamine and poly vinylpyrrolidone (PVP) reacted with neat sulfuric acid readily to form two new organic solid acids namely melamine-(H2SO4)3 and PVP-(H2SO4)n. These solid acids were used for the first nitration of bisphenol A as well as other phenols in the presence of NH4NO3. Mono- and di-nitro bisphenol A have been characterized with IR and 1H NMR techniques.