Creep Behavior and Microstructure Evolution of Sand–Cast Mg–4Y–2.3Nd–1Gd–0.6Zr Alloy Crept at 523–57

来源 :Journal of Materials Science & Technology | 被引量 : 0次 | 上传用户:aidam
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High temperature tensile–creep behavior of Mg–4Y–2.3Nd–1Gd–0.6Zr(wt%,WE43(T6)) alloy at 523–573 K was investigated.The creep stress exponent is equal to 4.6,suggesting the underlying dislocation creep mechanism.The activation energy is(199 ± 23) k J/mol,which is higher than that for selfdiffusion in Mg and is believed to be associated with precipitates coarsening or cross slip.The creep mechanism is further suggested to be dislocation climb at 523 K,while a cross slip at 573 K is possible.The metastable β′ and β1 phases in the WE43(T6) alloy were relatively thermal stable at 523 K and could be effective to hinder the dislocation climb,which contributed to its excellent creep resistance.However,at 573 K it readily transforms into equilibrium βe phase and coarsens within two hours,thereby causing a decrease of creep resistance.In addition,precipitate free zones approximately normal to applied stress direction(directional PFZs) developed during the creep deformation,especially at 573 K.Those zones became preferential sites to nucleate,extend and connect microcracks and cavities,which lead to the intergranular creep fracture.Improving the thermal stability of precipitates or introducing thermally stable fine plate-shaped precipitates on the basal planes of Mg matrix could enhance the high temperature creep resistance. Suggesting that the creep stress behavior of Mg-4Y-2.3Nd-1Gd-0.6Zr (wt%, WE43 (T6)) alloy at 523-573 K was investigated. The creep stress exponent is equal to 4.6, suggesting that the underlying dislocation creep mechanism. The activation energy is (199 ± 23) kJ / mol, which is higher than that for selfdiffusion in Mg and is believed to be associated with precipitates coarsening or cross slip. creep mechanism is further suggested to be dislocation climb at 523 K, while a cross slip at 573 K is possible. Metastable β ’and β1 phases in the WE43 (T6) alloy were relatively thermal stable at 523 K and could be effective to hinder the dislocation climb, which contributed to its excellent creep resistance Since, at 573 K it readily transforms into equilibrium βe phase and coarsens within two hours, thereby causing a decrease of creep resistance. In addition, precipitate free zones approximately normal to applied stress direction (directional PFZs) developed during the creep deformation, espe cially at 573 K. Thhose zones became preferential sites to nucleate, extend and connect microcracks and cavities, which lead to the intergranular creep fracture. Impinging the thermal stability of precipitates or incothermally stable fine plate-shaped precipitates on the basal planes of Mg matrix could enhance the high temperature creep resistance.
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