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六味地黄丸(浓缩)收载于卫生部药品标准第十一册(1993年),标准中采用薄层扫描法对其中主药山茱萸有效成分熊果酸进行定量,但操作繁琐,重现性差,我们采用HPLC-ELSD对制剂中熊果酸进行含量测定方法的研究。1实验方法与结果1.1仪器与试剂:美国ALLT
Liuwei Dihuang Pills (concentrated) is contained in the eleventh volume (1993) of the Ministry of Health’s Drug Standards. The thin-layer scanning method is used to quantify the active ingredient ursolic acid, but the operation is cumbersome and the reproducibility is poor. We used HPLC-ELSD to study the content of ursolic acid in the formulation. 1 Experimental methods and results 1.1 Instruments and reagents: United States ALLT