【摘 要】
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Synthesis of ligand, a -oxo-pentanedioic acid benzoyl hydrazone (H2LPB), and its six rare earth (La, Pr, Nd, Sm, Gd and Er) complexes are reported. The composit
【机 构】
：
Chemistry and Engineering College,Department of Physics,National Laboratory of Applied Organic Chemi
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Synthesis of ligand, a -oxo-pentanedioic acid benzoyl hydrazone (H2LPB), and its six rare earth (La, Pr, Nd, Sm, Gd and Er) complexes are reported. The composition and the properties of the complexes were characterized by element analysis, thermal analysis, UV, IR and 1H NMR spectra. Besides, relaxivity (R1) of Gd-complex has been determined by INVREC.Au program, using inversion recovery pulse sequences, R1=8.05 mmol.L-1.s-1. The acute toxicity of Gd-complex in animal has also been tested, and the median lethal dose (LD50) is equal to (468.2±30) mg/kg.
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