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目的:建立筋骨跌打丸质量标准。方法:通过TLC对筋骨跌打丸中橙皮苷、大黄进行鉴别;同时采用RP-HPLC法测定柚皮苷含量。结果:TLC色谱中均能检出橙皮苷、大黄;柚皮苷在0.1030~1.4420μg范围内具有良好线性关系(r=0.9999),平均回收率为:99.40%(RSD:1.77%)。结论:方法简单可靠,重现性好,可用于筋骨跌打丸的质量控制。
Objective: To establish the quality standard of bone bone drop pills. Methods: The identification of hesperidin and rhubarb in Jingu Guading Pills was performed by TLC. The content of naringin was determined by RP-HPLC. RESULTS: TLC could detect hesperidin and rhubarb. Naringin had good linearity in the range of 0.1030-1.4420 μg (r=0.9999). The average recovery rate was 99.40% (RSD: 1.77%). Conclusion: The method is simple, reliable and has good reproducibility. It can be used for the quality control of bone bone drop pills.