一种通用的微波化学合成实验装置

来源 :化学研究与应用 | 被引量 : 0次 | 上传用户:pangpanghai
下载到本地 , 更方便阅读
声明 : 本文档内容版权归属内容提供方 , 如果您对本文有版权争议 , 可与客服联系进行内容授权或下架
论文部分内容阅读
A household microwave oven can be modified not only to be able to regulate microwave power continuously (including the intensity of EM field in the cavity),but also to be able to fit three flasks into the cavity (each flask can be connected to a reflux condenser outside the cavity).The microwave heating uniformity of the three flasks was tested using water (50g. and 30g.) and ethanol (40g.) respectively.The results showed that the heating uniformity of the three flasks was 89±5% (average±σ n-1 ,n=22) and the microwave leakage was below 1 mW/cm 2.The modified oven was used by 90 undergraduate students for chemical synthesis experiment (microwave synthesis of veratraldehyde). The reaction time was only 2~3min.and the average yield was 86±9% (n=90).The variation of the average yields of among student groups was only 2%.Through variance analysis,F1,showing the difference was not significant.This modified microwave oven is especially suitable for chemical synthesis experiment for undergraduate students and for microwave digestion in analysis labs. A household microwave oven can be modified not only to be able to regulate microwave power continuously (including the intensity of EM field in the cavity), but also to be able to fit three flasks into the cavity (each flask can be connected to a cavity the microwave heating uniformity of the three flaksks was tested using water (50g. and 30g.) and ethanol (40g.) respectively.The results showed that the heating uniformity of the three flasks was 89 ± 5% ( the modified oven was used by 90 undergraduate students for chemical synthesis experiment (microwave synthesis of veratraldehyde). The reaction time was only 2 ~ 3min. And the average yield was 86 ± 9% (n = 90). The variation of the average yields of among students groups was only 2%. Through variance analysis, F1, showing the difference was not significant. This modified microwave oven is especially suitable for chemical synthesis experiment for undergraduate students and for microwave digestion in analysis labs.
其他文献
我国国画历史悠久,是我国优秀传统文化的结晶.笔墨,是创作国画过程中的关键要素,备受国画创作者的重视,并将其广泛应用于国画创作中.从某种角度来说,国画的灵魂和国画的神韵
银杏树系落叶乔木,为地球上存活最久的植物之一,有“活化石”之称。银杏叶始载于《本草品汇精要》,在中国传统中药中已运用数千年。据我国药典记载,银杏叶可润肺、平喘、止咳,用于
风景油画创作极具艺术性和观赏性,且油画专业在我国高校教育中也有了空前的发展,每年的报考人数和实际录取人数都在不断增长.生活水平的提高以及社会的发展,让人们对生活有了
近年来,学术界对儿童绘本创作的研究展开了大规模探究.随着对传统文化与艺术元素在绘本创作中的研究逐渐深入,可以发现在儿童绘本创作中有大量的造型、构图、色彩等绘画元素
八大山人能诗、书,也擅于画,其在中国画艺术上独具一格,可以说是全能且极为优秀的艺术家,让人们沉浸在他的艺术魅力之中.本文以八大山人绘画特点为切入点,通过层层推进,结合
吴昌硕是晚清民国时期中国最具影响力的画家,他的作品题材宽泛,其中包括了书法、绘画等内容.他不但继承了传统文人绘画的儒雅之风,也能顺应社会时势推移,反映生活,笔墨语言在
随着我国经济的飞速发展,人们的精神文化需求也逐渐提升,为博物馆发展带来广阔的发展机遇,在博物馆陈列展览活动增加的同时,也为博物馆陈列展档案工作带来巨大挑战.要想充分
公元916年,契丹首领耶律阿保机建立契丹国,公元947年改国号为辽.辽国版图十分广阔,可以覆盖当今的河北、山西、内蒙古及东北三省等大部分地区,其东西版图界线为黑龙江口及阿
中国特色社会主义文化事业正在全面推动文化自信的建立,确保中华优秀传统文化能够在中华民族伟大复兴的进程中发挥积极作用.非物质文化遗产的保护与传承是传统文化传播与文化
在我国,非物质文化遗产档案是非物质文化遗产得以传承的重要载体,属于一个民族、一个国家最为宝贵的记忆财富.就现代博物馆而言,积极开展非遗档案管理工作,需要充分发挥博物