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INTRODUCTION. Reaction of MoCl_3·3H_2O with dithio-carbamate to synthesize dinuclear or trinuclear molybdenum complexes is an interesting topic. We have obtained sulfido-bridged molybdenum(V) complex Mo_2(μ-S)_2O_2(S_2CNEt_2)_2 by reacting MoCl_3·3H_2O with NadtcEt_2 in MeOH solvent. The molecular structure of the title compound was characterized by, X-ray structure determination. We report the result of the structure determination in this paper.
INTRODUCTION. Reaction of MoCl_3 · 3H_2O with dithio-carbamate to synthesize dinuclear or trinuclear molybdenum complexes is an interesting topic. We have obtained sulfido-bridged molybdenum (V) complex Mo_2 (μ-S) _2O_2 (S_2CNEt_2) _2 byactive MoCl_3 · 3H_2O with NadtcEt_2 in MeOH solvent. The molecular structure of the title compound was characterized by, X-ray structure determination. We report the result of the structure determination in this paper.