Photochemical microfluidic synthesis of vitamin D3 by improved light sources with photoluminescent s

来源 :中国化学工程学报(英文版) | 被引量 : 0次 | 上传用户:zhanghao2018
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This study presents a novel technique for the controllable preparation of photoluminescent substrates to enhance the photochemical microfluidic synthesis of vitamin D3.The dip-coating method to prepare the substrates was experimentally optimized,and the corresponding emission behaviors were systematically investigated.The substrates were successfully used to enhance the ultraviolet B (UVB) emission of a low-power light source (eg.,an 8 W lamp),whose UVB emission intensity was increased by approximately 11 times.By virtue of the novel light source,the productivity of a single set of photochemical micro reactor with a 12-meter-long channel (0.6 mm i.d.) was increased to 1.83 kg·a-1,which was 42% higher than that of a 100 W lamp,and no cooling devices were used.The method is simple and has great potential to replace traditional medium-pressure mercury lamps for UVB-irradiated photochemical reactions.
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