【摘 要】
：
The compound phenol,2-[4(S)-4,5-dihydro-4-phenyl-2-ozazolinyl(1,C15H13NO2)was synthesized with a simple,one step method free of water and air.It was obtained in
【机 构】
：
Hefei University of Technology,University of Science and Technology
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The compound phenol,2-[4(S)-4,5-dihydro-4-phenyl-2-ozazolinyl(1,C15H13NO2)was synthesized with a simple,one step method free of water and air.It was obtained in a moderate yield from the reaction of 2-hydroxybenzonitrile with optically active amino alcohol in chlorobenzene under dry,anaerobic conditions.It belongs to the orthorhombic system,space group P212121with a=5.786(5),b=10.730(5),c=19.722(5)(A),C15H13NO2,Mr=239.26,V= 1224.4(12)(A)3,Z=4 and Dc=1.298 mg/m3.The final R=0.0324 for 1627 observed reflections with I > 2σ(I)and Rw= 0.0826 for all data.The structure of compound 1 was determined by X-ray diffraction,NMR and HRMS.
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