【摘 要】
：
hospho-olivine LiFePO has been prepared using a facile hydrothermal method by optimizing the reaction temperatures. Structural and morphological properties of t
【机 构】
：
State Key Laboratory of Structural Chemistry,Key Laboratory of Optoelectronic Materials Chemistry an
论文部分内容阅读
hospho-olivine LiFePO has been prepared using a facile hydrothermal method by optimizing the reaction temperatures. Structural and morphological properties of the as-prepared LiFePO powders are systematically characterized using X-ray diffraction (XRD), scanning electron microscopy (SEM), transmission electron microscopy (TEM), infrared spectra, UV-vis spectra, and Mossbauer spectroscopy. It is demonstrated that the samples prepared in the temperature range from 160 to 200 ℃ crystallize in a single phase of phospho-olivine structure. All particles are rod-like,showing dimensions of approximately 150～200 nm in width and 500～600 nm in length with apreferential growth direction of [001]. Within the lattice of LiFePO rods, Fe sites, which increases the cell volume. The electrochemical performance of LiFePO is investigated by charge/discharge experiments.It is found that LiFePO rods prepared at 200 ℃ deliver a specific discharge capacity of 147 mAh g disorderly occupying the Li
其他文献
The title compound (7R,8S,9S,12S)-13,14-dehydro-1-(4-fluorobenzyloxy)-N-methyl-2,13-dimethoxy-12-hydroxymorphinane was synthesized by the reaction of O-4-bromob
A series of glucose-cholesterol derivatives 8a-8e as ligands for brain targeting liposomes were synthesized. The preparation of compound 6 involved temporary pr
We studied the co-adsorption of hydrogen molecule and ions (Li, K, Mg, Ca) insidethe single-waUed carbon nanotubes (SWNTs) by using density-functional theory (D
The title compound 2-amino-4-(4-hydroxy-3,5-dimethoxyphenyl)-5-methyl-6-phenyl nicotinonitrile, CHNO,was synthesized via four-component reactions between propio
An iron(Ⅱ) formate [HCO][Fe(HCO)] (1)has been synthesized under hydro-thermal conditions and characterized by single-crystal X-ray diffraction analysis. Comple
Hydrothermal reaction of MgCl and ethyl tetrazolate-5-carboxylate at 160 ℃unexpectedly yielded compound {(HO)[Mg(HO)]CI} (1). The result of Ⅹ-ray diffraction
Fly ash was used as a low-cost adsorbent for removing dissolved organic matter (DOM) in secondary effluent.Batch experiments were conducted under various adsorb
One novel entangled cobalt compound, {[Co(nbta)(4,4-bpy)(HO)](HO)}n (1,Hnbta=5-nitro-1,2,3-benzenetricarboxylic acid, 4,4-bpy = 4,4-bipyridyl), was prepared and
现今科学技术发展的突飞猛进，电动机及控制设备的技术性能也日益完善。在工作中如何正确的使用和掌握其性能，还需要我们在实际工作中不断积累经验，判断电动机及控制设备存在的问
从脱盐水处理工艺、投资、运行成本和环保等方面,对离子交换处理方案与膜法处理方案进行了经济技术比较.