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在氢氧化钾存在下,已内酰胺与氯代十二烷在二甲基亚砜溶剂中,可顺利的进行 N—烃苍化反应,收率可达63%。用气相色谱测定,含量为98.5%,符合卫生部药品标准 WS-128-87标准要求.
In the presence of potassium hydroxide, caprolactam and chlorododecane in dimethyl sulfoxide solvent, N-hydrocarbon can be smoothly carried out the reaction, the yield of up to 63%. Determination by gas chromatography, the content of 98.5%, in line with the Ministry of Health Drug Standards WS-128-87 standard requirements.