Structural and magnetic properties of Sm(Co_(0.7)Fe_(0.1)Ni_(0.12)Zr_(0.04)B_(0.04))_(7.5) melt spun

来源 :Journal of Rare Earths | 被引量 : 0次 | 上传用户:ktcalf
下载到本地 , 更方便阅读
声明 : 本文档内容版权归属内容提供方 , 如果您对本文有版权争议 , 可与客服联系进行内容授权或下架
论文部分内容阅读
We investigated the structural and magnetic properties of Sm(Co0.7Fe0.1Ni0.12Zr0.04B0.04)7.5 melt spun ribbons. Samples were arc melted then melt spun at 37 m/s up to 55 m/s to obtain ribbon for powdering. Annealing was performed in argon atmosphere for 30- 75 min at 600-870 oC. In as-spun ribbons the hexagonal SmCo7 (TbCu7-type of structure) of crystal structure was determined from x-ray diffraction patterns, while fcc-Co has been identified as a secondary phase. After annealing, the 1:7 phase of the as-spun ribbons transformed into 2:17 and 1:5 phases. X-ray patterns for as-milled powders exhibited very broad peaks making it difficult to identify a precise structure but repre-sented the 1:7 structure after annealing at low temperature (650 oC). TEM analysis showed a homogeneous nanocrystalline microstructure with average grain size of 30-80 nm. Coercivity values of 15-27 kOe were obtained from hysteresis loops traced up to a field of 5 T. The co-ercivity decreased as temperature increases, but it maintained values higher than 5 kOe at 380 oC. The maximum energy product at room temperature increased, as high as 7.2 MGOe, for melt-spun isotropic ribbons produced at higher wheel speeds. Anisotropic ribbons had a maximum energy product close to 12 MGOe. We investigated the structural and magnetic properties of Sm (Co0.7Fe0.1Ni0.12Zr0.04B0.04) 7.5 melt spun ribbons. Samples were arc melted then melt spun at 37 m / s up to 55 m / s to obtain ribbon for powdering . Annealing was performed in argon atmosphere for 30-75 min at 600-870 oC. In as-spun ribbons the hexagonal SmCo7 (TbCu7-type of structure) of crystal structure was determined from x-ray diffraction patterns, while fcc-Co has been identified as a secondary phase. After annealing, the 1: 7 phase of the as-spun ribbons transformed into 2:17 and 1: 5 phases. X-ray patterns for as-milled powders coated very broad peaks making it difficult to identify a precise structure but repre- sented the 1: 7 structure after annealing at low temperature (650 oC). TEM analysis showed a homogeneous nanocrystalline microstructure with average grain size of 30-80 nm. Coercivity values ​​of 15-27 kOe were obtained from hysteresis loops traced up to a field of 5 T. The co-ercivity decreased as temperature incr eases, but it maintained values ​​higher than 5 kOe at 380 oC. The maximum energy product at room temperature increased, as high as 7.2 MGOe, for melt-spun isotropic ribbons produced at higher wheel speeds. Anisotropic ribbons had a maximum energy product close to 12 MGOe.
其他文献
2007年1月1日,在白雪茫茫的九龙国际滑雪场,由山西省旅游局、省体育局共同主办,旅游时代杂志社、九龙国际滑雪场等单位共同承办的“奥运北京大运山西·2007山西(奥运)旅游宣
Multicolor luminescent rare-earth ion-doped Y2O3 nanocrystals(NCs) were prepared by a solvethermal method.The as-synthesized NCs yielded nanosheets,nanowires(NW
Ionic liquids (ILs) have been widely used in separation, catalysis, electrochemistry, etc., and one of the most outstanding characteristics is that ILs can be t
本文建立了用微波消解-原子荧光光谱法测定人工养殖甲鱼中的金属汞,确定了消解试剂为3:2的硝酸和双氧水,原子荧光的还原剂为0.05%的硼氧化钾,酸度为1%的盐酸。用以上最优化条
《北京水务》获由中共北京市委宣传部、北京市人事局、北京市新闻出版局共同颁发的第二届“北京市优秀出版物奖”子奖“北京市优秀期刊奖”。在9月15日的第七届北京图书节上
不知道Chand先生对生在西班牙留下举世瞩目建筑的高第有多少了解,因为他们采用的是两种相同的材料:石头和碎瓷片。为了构造他梦想天国中的天子神女,Chand每天在城里到处收集
关于图书馆学的研究对象,我国图书馆学界40年来(1949—1989)进行过热烈争鸣,共发表论文70篇,有20种专著涉及到。这些论著中约有60种不同观点,其中有代表性的观点有11种。即:
(Fe50Co25B15Si10)80Cu20 ribbons are prepared by using the single-roller melt-spinning method.A dual-layer structure consisting of a(Fe,Co)-rich amorphous phase
The additives-doped α-nickel hydroxides were prepared by supersonic co-precipitation method. The crystal structure and grain size of the prepared samples were
河南的手足口病疫情为何继2009年的暴发后,再次大面积蔓延? 曾在2008、2009年两度凶猛来袭的手足口病,正再度攻击中国。卫生部新闻发言人邓海华4月13日称,截至到4月11日,201