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采用气提吸附/热脱附/气相色谱-质谱法对齐鲁公司所处地区工业污水进行分析。方法采用Tenax-GC吸附剂对样品进行气提吸附,脱附时样品直接进入色谱仪汽化室,一次进样即可完成全组分分析,共检测出含四氯丙醚在内的40种有机组分,测定了各组分的程序升温保留指数。气相色谱-质谱法测定出四氯丙醚三个异构体的结构。
Adsorption / desorption / gas chromatography-mass spectrometry was used to analyze the industrial wastewater in Qilu Company. Methods Tenax-GC adsorbent was used to conduct gas-lift adsorption. When desorption, the sample directly entered the gas chromatograph vaporization chamber. The complete component analysis was completed in one injection. A total of 40 organic compounds Components, determination of each component of the program temperature retention index. The structure of three isomers of tetrachloropropyl ether was determined by gas chromatography-mass spectrometry.