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A planar metal complex NiL,H2L = acenaphthenequinone bis(S-benzyldithiocarbazate),1,has been prepared via the template effect of nickel ion.Crystal structure of 1 was determined by X-ray diffraction analysis and shows the planar coordination configuration around the central nickel atom.Z-scan measurements show that 1 is a transition metal complex exhibiting high third-order nonlinear optical effect.