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A novel 2-D supramolecular network formed by the Fe3O building unit through three hydrogen bonds [Fe3O (O2CCH2OC6H5)6(3H2O)]NO3·2H2O (1) are presented. The title complex crystallizes in monoclinic, space group P21/n, with a=1.709 3(2) nm, b=3.1529(3)