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The title compound,[Ni(C8N3H7)3]4[Mo8O26]2·6H2O 1,has been synthesized from the reaction of 2-(1H-pyrazol-3-yl)-pyridine (L) with (NH4)2MoO4·2H2O and NiCl2·6H2O. Elemental analysis,IR,UV spectra and X-ray single-crystal diffraction were car