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Prior to formation of the micelles of cationic surfactant (CSF). bromopyrogallol red (BPR) could exist in the forms of both monomer and ollgomer. After that, however. only BPR monomer existed. Nonionic surfactant OP-10 favoured the oligomerthetion of BPR monomer.The mixed micellar media prepared by mixing CSF and OP-10 in an appropriate ratio could be used for the sensitive and selective determination of Mo in Mo/W binary mixtures